Synthesis of novel Fe3O4 nanostructures surrounded by Ti-MOF nanostructures as bioactive and efficient catalysts in three-component synthesis of new pyrazole derivatives

Synthesis and reporting of new nanoparticles with diverse properties is important in chemistry. A one-step, rapid controllable synthesis the Fe 3 O 4 surrounded Ti-MOF nanostructures was carried out microwave technology. After identifying confirming structure, used as a suitable catalyst high thermal resistance recyclable three-component reaction phenylhydrazine, malononitrile aldehyde to novel pyrazole derivatives. Continuing investigations on nanostructures, its antimicrobial were tested Gram-positive bacterial species, Gram-negative species fungi bacterial. Identification morphology size distribution technique (SEM), surface area (BET), Infrared spectroscopy (FT-IR), Energy-Dispersive X-ray (EDX/EDX mapping), Vibrating Sample Magnetometer (VSM) performed. Synthesized derivatives than previously reported methods have less time efficiency. In effects observed based MIC, MBC, MFC values.